9001cc½ðɳÒÔ³ÏΪ±¾

ÊÖ³Öʽ¹âÆ×ÒÇÊÖ³ÖʽºÏ½ðÆÊÎöÒǺϽðÆÊÎöÒÇ
¹ÉƱ´úÂ룺300165 ÆóÒµÓÊÏä Ͷ×ÊÕß¹ØÏµ
9001cc½ðɳÒÔ³ÏΪ±¾(Öйú)ÓÐÏÞ9001cc½ðɳÒÔ³ÏΪ±¾¹«Ë¾

ʳÎïÇå¾²

ÄúÄ¿½ñËùÔÚÒ³£ºÊ×Ò³ > ½â¾ö¼Æ»® > ʳÎïÇå¾²

¸ß¾«¶ÈË®ÖÊÖØ½ðÊôICPMSÔÚÏß¼à²âϵͳ²â¶¨ÉúÑÄÒûÓÃË®ÖеÄÍ­¡¢Éé¡¢ÌࡢǦ¡¢¹¯µÈ¶þÊ®¶àÖÖ½ðÊôÔªËØ

Ðû²¼ÈÕÆÚ£º2020/8/11 9:05:25  µã»÷´ÎÊý£º47434

Ëæ×ÅÎÒ¹úÉç»á¾­¼ÃµÄÉú³¤ÒÔ¼°¹¤ÒµÊÖÒÕµÄһֱˢУ¬ÇéÐÎÎÛȾÈÕÒæÑÏÖØ£¬ÓÈÆäÊÇË®ÌåÖØ½ðÊôµÄÎÛȾÎÊÌ⣬ÒѾ­³ÉΪµ±ÏÂÉç»á×îÊÜÈÈÒéµÄ»°ÌâÖ®Ò»¡£ÓÅÒìµÄË®ÇéÐΣ¬²»µ«ÊÇÈËÀàÉúÑĵĻù±¾°ü¹Ü£¬Ò²ÊÇÉç»áÒ»Á¬Éú³¤µÄ»ù´¡¡£9001cc½ðɳÒÔ³ÏΪ±¾ÒÇÆ÷¾­Óɺã¾ÃµÄÑо¿¼°ÐÔÄܲâÊÔ£¬ÃæÁÙÇéÐα£»¤¼à²âÍÆ³öÁËÒ»¿îȫеÄË®ÖÊÔÚÏß¼à²âϵͳ£¨POW-I£©¡£

POW-IÒÀÍеç¸ÐñîºÏµÈÀë×ÓÌåÖÊÆ×ÒÇ£¨ICP-MS 2000ϵÁУ©£¬½ÓÄÉÒ»Ì廯¡¢¼¯³ÉÁª¶¯µÄÔËÐз½·¨£¬ÓÃÏÖ´úÐÅÏ¢ÊÖÒÕ¾ÙÐÐÊý¾ÝÊÕÂÞ¡¢Êý¾Ý´¦Öóͷ££¬¾ßÓÐ×Ô¶¯È¡Ë®¡¢×Ô¶¯¹ýÂË¡¢×Ô¶¯ÑùÆ·´¦Öóͷ£¡¢×Ô¶¯Êý¾ÝÊÕÂÞ¡¢×Ô¶¯ÖÊÁ¿¿ØÖÆ¡¢×Ô¶¯Êý¾Ý´«ÊäµÈ¹¦Ð§¡£È«ÏµÍ³½ÓÄÉÄ£¿é»¯Éè¼Æ£¬Î¬»¤¼òÆÓ±ã½Ý£¬¾ßÓжàÔªËØÍ¬Ê±¼à²â¡¢×Ô¶¯Ô¤¾¯¼°Êý¾ÝÒì³£´¦Öóͷ£¡¢ÆÊÎöËÙÂʿ졢¼ì³öÏ޵͵ÈÌØµã¡£

±¾ÎIJο¼ÇéÐα£»¤²¿Ðû²¼µÄ¡¶ HJ 700-2014Ë®ÖÊ65ÖÖÔªËØµÄ²â¶¨ µç¸ÐñîºÏµÈÀë×ÓÌåÖÊÆ×·¨¡·£¬½ÓÄÉRh¡¢Re×÷ÄÚ±ê,¶ÔijÒûÓÃˮԴµØË®ÑùÖеÄÍ­¡¢Éé¡¢ÌࡢǦ¡¢¹¯µÈ¶þÊ®¶àÖÖ½ðÊôÔªËØ¾ÙÐмà²â£¬ÊµÑéЧ¹ûÅú×¢¸ÃϵͳÄܹ»¿ìËÙ¡¢×¼È·µÄÖª×ãË®ÖÊÆÊÎöµÄÒªÇó¡£


1. ϵͳ¼ò½é

POW-IÊǼ¯×Ô¶¯¼à²âºÍ×Ô¶¯ÆÊÎöΪһÌåµÄµÄÊý×Ö»¯¹ÜÀíÆ½Ì¨,ÊÇÖúÁ¦ÇéÐα£»¤ÐÐÒµºÍ°ëµ¼ÌåÐÐҵʵÏÖË®ÖÊî¿ÏµµÄÖ÷Òª¹¤¾ß¡£

9001cc½ðɳÒÔ³ÏΪ±¾(Öйú)ÓÐÏÞ9001cc½ðɳÒÔ³ÏΪ±¾¹«Ë¾

ͼ1. POW-I ¸ß¾«¶ÈË®ÖÊÖØ½ðÊôICPMSÔÚÏß¼à²âϵͳ

2. ²âÊÔÔ­Àí

POW-Iͨ¹ý²ÉË®×°Öý«Ë®ÑùËÍÈëǰ´¦Öóͷ£Ä£¿é£¬¾­Ëữ»òÏû½âºóÔÚ¶àͨ·§µÄ×÷ÓÃÏÂͨ¹ýÈ䶯±Ã½øÈëICP-MSϵͳ¾ÙÐÐÆÊÎö¡¢¼ì²â£¬»ñµÃ×îÖÕÊý¾Ý£¬¾­Èí¼þ´¦Öóͷ£ÏµÍ³ÉÏ´«ÖÁ¿Í»§¶Ë»òÔÆÆ½Ì¨¡£

3. ʵÑ鲿·Ö

3.1 ʵÑéËùÓÃ×°±¸¼°ÊÔ¼Á

¸ß¾«¶ÈË®ÖÊÔÚÏßϵͳ£¨POW-I£¬9001cc½ðɳÒÔ³ÏΪ±¾£©£»

ʵÑéËùÓó¬´¿Ë®£¨µç×èÂÊ´ï18.25M¦¸¡¤cm£¬Ä¬¿ËÃÜÀí²©£¬µÂ¹ú£©£»

Ïõ ËᣨÖÊÁ¿±ÈΪ65%£¬G.R£¬ÈøÀÍ£¬Î÷°àÑÀ£©£»

¶àÔªËØ±ê×¼ÈÜÒº£¨10mg/L£¬Inorganic Ventures£¬ÃÀ¹ú£©£»

AuÔªËØ±ê×¼ÈÜÒº£¨1000mg/L£¬¹ú¼ÒÓÐÉ«½ðÊô¼°µç×ÓÖÊÁÏÆÊÎö²âÊÔÖÐÐÄ£©£»

ë² Æø£¨´¿¶È99.999%£¬Air Products£¬ÃÀ¹ú£©£»

ÇéÐζàÔªËØ½ðÊô»ì±ê£¨BYT400043/B2003238,100¡À10 ?g/L¼°20.0¡À2 ?g/L£¬±±¾©Ì³Ä«ÖÊ¼ì¿Æ¼¼ÓÐÏÞ¹«Ë¾£©£»

ÇéÐαê×¼ÎïÖÊË®ÖÊÅð£¨BY400156/B1905153,0.819¡À0.036 mg/L,±±¾©Ì³Ä«ÖÊ¼ì¿Æ¼¼ÓÐÏÞ¹«Ë¾)£»

ÇéÐαê×¼ÎïÖÊË®Öʹ¯£¨BY400030/B191249,4.23¡À0.62 ?g/L£¬±±¾©Ì³Ä«ÖÊ¼ì¿Æ¼¼ÓÐÏÞ¹«Ë¾£©¡£

3.2 ±êÒºÅäÖÆ

ÅäÖÆ²î±ðŨ¶ÈÌݶÈBe¡¢B¡¢Al¡¢Ti¡¢V¡¢Cr¡¢Mn¡¢Fe¡¢Co¡¢Ni¡¢Cu¡¢Zn¡¢As¡¢Se¡¢Mo¡¢Ag¡¢Cd¡¢Sb¡¢Ba¡¢Hg¡¢Tl¡¢Pb¶àÔªËØ»ìÏý±ê×¼ÈÜÒº£¬ÓÚһϵÁÐ500mLµÄPFAÆ¿ÖУ¬Í¬Ê±»®·Ö¼ÓÈë200¦Ìg/L½ð±ê×¼ÈÜÒº£¬ÆäÄ¿µÄÊǰü¹ÜHgµÄÎȹÌÐÔ¡£Í¬Ê±ÓÃ1%µÄÏõËá¾ÙÐж¨ÈÝ£¬ÄÚ±êÔªËØRh¡¢ReÒÔÔÚÏßÈýͨ·½·¨¾ÙÐмÓÈ룬ĸҺŨ¶ÈΪ82.2¦Ìg/L£¬ÕÛËã³É×îÖÕŨ¶ÈΪ10.0¦Ìg/L£¬Åä֯ō¶ÈÈç±í1¡£

±í1. ¸÷ÔªËØ±ê×¼ÈÜҺŨ¶È£¨?g/L£©

ÔªËØ

±êÒº1

±êÒº2

±êÒº3

±êÒº4

±êÒº5

±êÒº6

Be¡¢Cd

1.0

2.0

5.0

10.0

20.0

50.0

B¡¢Al¡¢Ti¡¢Zn¡¢Ba

5.0

10.0

20.0

50.0

100

200

V¡¢Cr¡¢Mn¡¢Fe¡¢Co¡¢Ni¡¢Cu¡¢
As¡¢Se¡¢Mo¡¢Ag¡¢Sb¡¢Tl¡¢Pb

1.0

5.0

10.0

20.0

50.0

100

Hg

0.50

1.0

2.0

3.0

4.0

5.0

3.3 ÔÚÏßÒÇÆ÷ÊÂÇé²ÎÊýÓÅ»¯£º

½ÓÄÉ10¦Ìg/L Li¡¢Co¡¢In¡¢Ce¡¢U ¾ÙÐÐ×Ô¶¯µ÷г£¬ËùµÃÔÚÏßÒÇÆ÷ÊÂÇé²ÎÊýÈç±í2¡£ 

±í2. ÔÚÏßÒÇÆ÷ÊÂÇé²ÎÊý

ÒÇÆ÷²ÎÊý

ÊÂÇéÌõ¼þ

 ÒÇÆ÷²ÎÊý

ÊÂÇéÌõ¼þ

RFµçÔ´¹¦ÂÊ

1300W

µÈÀë×ÓÆø

13L/min

¸¨ÖúÆøÁ÷ËÙ

  1.06 L/min

ÔØ  Æø

1.2L/min

²ÉÑùÉî¶È

16

ɨÃè·½·¨

Ìø ·å

                                              

3.4 ʵÑéÊý¾Ý

3.4.1 ÒªÁì¼ì³öÏÞ

´ýÒÇÆ÷ÈÈ»úÍê³Éºó£¬±êÒº¼°ÑùÆ·ÔÚÈ䶯±ÃµÄ×÷ÓÃÏ£¬»®·Öͨ¹ý¸÷×ÔͨµÀ½øÈëICP-MSÆÊÎöÒÇ£¬»ñµÃ±ê×¼ÇúÏß¡£¶ÔÑùÆ·¿Õȱ¾ÙÐÐÖØ¸´²â¶¨11´Î£¬ÒÔ3±¶µÄ±ê×¼Îó²îËù¶ÔÓ¦µÄŨ¶È£¬×÷Ϊ±¾ÒªÁìÖи÷ÔªËØµÄ¼ì³öÏÞ£¬ÒÔ10±¶µÄ±ê×¼Îó²îËù¶ÔŨ¶È£¬ÕÛËãΪ±¾ÒªÁìµÄ²â¶¨ÏÂÏÞ£¬Èç±í3Ëùʾ¡£

 ±í3. ¸÷ÔªËØµÄ¼ì³öÏÞ£¨?g/L£©

ÔªËØ

¼ì³öÏÞ

ÔªËØ

¼ì³öÏÞ

Be

0.01

B

0.30

Al

0.19

Ti

0.41

V

0.06

Cr

0.05

Mn

0.04

Fe

2.88

Co

0.01

Ni

0.06

Cu

0.08

Zn

0.32

As

0.10

Se

0.50

Mo

0.02

Ag

0.03

Cd

0.01

Sb

0.15

Ba

0.05

Hg

0.05

Tl

0.01

Pb

0.02        


3.4.2 ÖÊ¿ØÑù²âÊÔ

¼ì³öÏÞ²âÊÔÍê³Éºó£¬¶ÔÅ𡢸õ¡¢Äø¡¢ÌàµÈ19ÖÖÇéÐαê×¼ÎïÖÊ£¨ÖÊ¿ØÑù£©Öظ´²â¶¨6´Î£¬È¡Æäƽ¾ùÖµ×÷ΪÔÚÏßÒÇÆ÷µÄ²â¶¨Öµ£¬Í¬Ê±ÅÌËãÆäϸÃܶȣ¨RSD£©£¬Èç±í4¡£

±í4. ÖÊ¿ØÑù¼°Ï¸Ãܶȣ¨n=6)

ÔªËØ

ÖÊ¿ØÑù£¨?g/L£©

RSD

(%)

ÔªËØ

ÖÊ¿ØÑù£¨?g/L£©

RSD

(%)

±ê×¼Öµ

²â¶¨Öµ

±ê×¼Öµ

²â¶¨Öµ

Be

20.0¡À2

20.0

3.40

B

819¡À36

824

1.05

V

20.0¡À2

19.6

1.58

Ti

20.0¡À2

21.8

2.77

Mn

100¡À10

98.1

1.92

Cr

20.0¡À2

20.7

0.96

Co

20.0¡À2

20.6

0.61

Fe

100¡À10

99.7

2.09

Cu

20.0¡À2

19.9

1.93

Ni

20.0¡À2

19.7

0.65

As

20.0¡À2

21.5

0.65

Se

20.0¡À2

21.4

2.67

Mo

20.0¡À2

20.1

3.47

Cd

20.0¡À2

19.0

1.07

Sb

20.0¡À2

20.4

1.02

Ba

20.0¡À2

20.7

1.55

Hg

4.23¡À0.62

4.56

1.47

Tl

20.0¡À2

20.3

1.70

Pb

20.0¡À2

19.4

1.90

/

/

/

/

3.4.3 ÏÖʵˮÑù¼°¼Ó±ê²âÊÔ

¶ÔÏÖʵˮÑù¾ÙÐÐÖØ¸´²â¶¨6´Î£¬È¡Æäƽ¾ùÖµ×÷ΪΪˮÑù²â¶¨Öµ£¬Í¬Ê±¶ÔË®Ñù¾ÙÐÐ¼Ó±êÆ½Ðвⶨ£¬ÅÌËãÆä¼Ó±ê½ÓÄÉÂÊ£¬Èç±í5Ëùʾ¡£

±í5. Ë®Ñù²â¶¨Öµ¼°¼Ó±ê½ÓÄÉÂÊ£¨n=6)

ÔªËØ

±¾µ×Öµ£¨?g/L£©

¼Ó±êÖµ£¨?g/L£©

²â¶¨Öµ£¨?g/L£©

½ÓÄÉÂÊ£¨%£©

Be

ND

1.0

1.04

104.0

B

9.13

50.0

64.23

110.2

Al

36.32

50.0

96.68

120.7

Ti

ND

50.0

50.62

101.2

V

0.23

5.0

4.77

90.8

Cr

0.20

10.0

10.21

100.1

Mn

2.31

10.0

11.72

94.1

Fe

431.10

100.0

537.80

106.7

Co

0.04

10.0

10.59

105.5

Ni

0.58

5.0

5.44

97.2

Cu

0.29

10.0

10.52

102.3

Zn

ND

50.0

45.69

91.4

As

ND

10.0

10.19

101.9

Se

ND

10.0

10.30

103.0

Mo

0.74

5.0

5.59

97.0

Ag

ND

5.0

4.77

95.4

Cd

ND

5.0

4.65

93.0

Sb

0.47

1.0

1.44

97.0

Ba

10.79

50.0

60.17

98.8

Hg

ND

0.20

0.24

120.0

Tl

ND

1.0

0.94

94.0

Pb

ND

10.0

10.12

101.2


3.5 Ч¹ûÓëÆÊÎö

Óɱí3¿ÉÖª£¬ÒªÁì¼ì³öÏÞÔÚ0.01¦Ìg/L~2.88¦Ìg/LÖ®¼ä¡£Æ¾Ö¤±¾ÒªÁìͬʱ¶ÔÇéÐαê×¼ÎïÖʵÄÍ­¡¢Éé¡¢ÌࡢǦ¡¢¹¯µÈ19ÖÖÔªËØ¾ÙÐмà²â£¬ÆäЧ¹ûÓë±ê×¼ÖµÍêÈ«ÎǺÏ£¬Ïê¼û±í4¡£

ËæºóʹÓÃPOW-I¶ÔÏÖʵˮÑù¾ÙÐÐÁ˼à²â£¬ÅÌËãÆä´ý²âË®ÑùµÄ¼Ó±êÂÊΪ90.8%~120.7%£¬Ï¸ÃܶÈΪ0.65%~3.47%£¬Ïê¼û±í4¡¢±í5¡£

4.½áÂÛ

±¾ÎIJο¼¡¶JJF 1565-2016¡·ºÍ ¡¶HJ 700-2014¡·±ê×¼£¬Ê¹Óø߾«¶ÈË®ÖÊÔÚÏßϵͳ£¨POW-I£©£¬¶ÔijµØÉúÑÄÒûÓÃË®ÖеÄÍ­¡¢Éé¡¢ÌࡢǦ¡¢¹¯µÈ¶þÊ®¶àÖÖ½ðÊôÔªËØº¬Á¿¾ÙÐмà²â£¬½ÓÄÉRh¡¢Re×÷ΪÄÚ±êÀ´Ð£ÕýÒÇÆ÷²¨¶¯ºÍ»ùÌåÓ°Ï죬Ч¹ûÅú×¢¸ÃÒªÁì¼ì³öÏ޵ͣ¬²âÊÔЧ¹û׼ȷ£¬¼Ó±ê½ÓÄÉÂʸߣ¬ÎȹÌÐԺã¬Óë¹Å°åµÄË®ÖÊÔÚÏßÒÇÆ÷Ïà±È£¬Ô½·¢¿ìËÙ±ã½Ý¡¢¿É¶àÔªËØÍ¬Ê±¼à²â£¬´ó´óµØÌá¸ßÁËË®Öʼà²âµÄЧÂÊ¡£ÓÉÒÔÉÏÊý¾Ý¿ÉÖª£¬POW-IÍêÈ«¿ÉÒÔÖª×ãÔÚÏßË®ÖÊÖжàÔªËØ¿ìËÙ¶¨ÐÔ¶¨Á¿ÆÊÎöµÄÒªÇó¡£

5.²Î¿¼ÎÄÏ×

[1] ÇéÐα£»¤²¿£¬HJ 700-2014 Ë®ÖÊ65ÖÖÔªËØµÄ²â¶¨£¬µç¸ÐñîºÏµÈÀë×ÓÌåÖÊÆ×·¨£¬ÖйúÇéÐοÆÑ§³öÊéÉ磬2014¡£

[2] ¹ú¼ÒÖÊÁ¿¼àÊÓÄ¥Á·¼ìÒß×ܾÖ£¬JJF 1565-2016 ÖØ½ðÊôË®ÖÊÔÚÏ߯ÊÎöÒÇУÑ鹿·¶£¬ÖйúÖʼì³öÊéÉ磬2016¡£

Ïà¹Ø²úÆ·

ÁªÏµ9001cc½ðɳÒÔ³ÏΪ±¾

Ïàʶ¸ü¶àÏêϸÐÅÏ¢£¬ÇëÖµç
400-7102-888
·ÇÊÂÇéʱ¼ä·þÎñÈÈÏß
139 1323 1381
¸øÎÒÃÇÁôÑÔ
ÔÚÏßÁôÑÔ
΢ÐÅÊÛºó·þÎñ¶þάÂë

ÍøÕ¾µØÍ¼